Technology Process of Potassium perfluorooctanoxyacetate
There total 3 articles about Potassium perfluorooctanoxyacetate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) tris(dimethylamino)sulfonium difluorotrimethylsilicate / 1.) acetonitrile, r.t., 2.) r.t., overnight
2: 78 percent / 0.8202 N aq. potassium hydroxide / ethanol / 2 h / Heating
With
potassium hydroxide; tris(dimethylamino)sulfonium trimethylsilyldifluoride;
In
ethanol;
DOI:10.1016/S0022-1139(00)80195-5
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 55 percent / sulfur tetrafluoride / bis-(2-methoxy-ethyl) ether / 1 h / Heating
2: 1.) tris(dimethylamino)sulfonium difluorotrimethylsilicate / 1.) acetonitrile, r.t., 2.) r.t., overnight
3: 78 percent / 0.8202 N aq. potassium hydroxide / ethanol / 2 h / Heating
With
potassium hydroxide; sulfur tetrafluoride; tris(dimethylamino)sulfonium trimethylsilyldifluoride;
In
ethanol; diethylene glycol dimethyl ether;
DOI:10.1016/S0022-1139(00)80195-5
