2,4,6-tris[p-(2,2'-dipyridylamino)phenyl]-1,3,5-triazine

Base Information

• Chemical Name: 2,4,6-tris[p-(2,2'-dipyridylamino)phenyl]-1,3,5-triazine
• CAS No.: 432551-44-5
• Molecular Formula: C₅₁H₃₆N₁₂
• Molecular Weight: 816.927
• Mol file: 432551-44-5.mol

Synonyms:

Chemical Property of 2,4,6-tris[p-(2,2'-dipyridylamino)phenyl]-1,3,5-triazine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 2,4,6-tris[p-(2,2'-dipyridylamino)phenyl]-1,3,5-triazine

There total 1 articles about 2,4,6-tris[p-(2,2'-dipyridylamino)phenyl]-1,3,5-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

di(pyridin-2-yl)amine (1202-34-2) + 2,4,6-tris(4-bromophenyl)-1,3,5-triazine (30363-03-2) → 2,4,6-tris[p-(2,2'-dipyridylamino)phenyl]-1,3,5-triazine (432551-44-5)

Guidance literature:

With potassium carbonate; copper(II) sulfate; at 210 ℃; for 8h;

DOI:10.1039/b105422h

Reference yield: 55.0%

[(PtPh2(μ-SMe2))n] + 2,4,6-tris[p-(2,2'-dipyridylamino)phenyl]-1,3,5-triazine (432551-44-5) → Pt3Ph6[2,4,6-tris[p-(2,2'-dipyridylamino)]phenyl]-1,3,5-triazine]

Guidance literature:

In tetrahydrofuran; mixt. of ligand and Pt-complex was dissolved in THF, stirred at room temp. for 30 min, stirred for 5 h at room temp.; filtered, dissolved in CH2Cl2, toluene was layered, solvent was allowed to diffuse, evapd. slowly over several d at ambient temp.; elem. anal.;

DOI:10.1021/om030262k

upstream raw materials:

di(pyridin-2-yl)amine

2,4,6-tris(4-bromophenyl)-1,3,5-triazine

Refernces