C₂₄H₂₈N₄O₅S₂

Base Information

• Chemical Name: C₂₄H₂₈N₄O₅S₂
• CAS No.: 1581769-15-4
• Molecular Formula: C₂₄H₂₈N₄O₅S₂
• Molecular Weight: 516.642
• Mol file: 1581769-15-4.mol

Synonyms:

Chemical Property of C₂₄H₂₈N₄O₅S₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₂₈N₄O₅S₂

There total 3 articles about C₂₄H₂₈N₄O₅S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-cyclopropyl-4-nitrobenzenesulfonamide (549476-61-1) → C24H28N4O5S2 (1581769-15-4)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium carbonate; [2,2]bipyridinyl; oxygen; copper diacetate / acetonitrile / 20 - 55 °C / Inert atmosphere

2: potassium hydroxide

With [2,2]bipyridinyl; oxygen; copper diacetate; sodium carbonate; potassium hydroxide; In acetonitrile; 1: |Chan-Lam Coupling;

DOI:10.1021/op500031z

Reference yield:

4-Nitrobenzenesulfonyl chloride (98-74-8) → C24H28N4O5S2 (1581769-15-4)

Guidance literature:

Multi-step reaction with 3 steps

1.1: toluene / 0.25 h / 0 - 15 °C / Inert atmosphere

1.2: 5 - 25 °C / Inert atmosphere

1.3: 4 h / 20 - 25 °C / Inert atmosphere

2.1: sodium carbonate; [2,2]bipyridinyl; oxygen; copper diacetate / acetonitrile / 20 - 55 °C / Inert atmosphere

3.1: potassium hydroxide

With [2,2]bipyridinyl; oxygen; copper diacetate; sodium carbonate; potassium hydroxide; In toluene; acetonitrile; 2.1: |Chan-Lam Coupling;

DOI:10.1021/op500031z

Reference yield:

N,N-dicyclopropyl 4-nitrobenzenesulfonamide (1581769-09-6) → C24H28N4O5S2 (1581769-15-4)

Guidance literature:

With potassium hydroxide;

DOI:10.1021/op500031z

upstream raw materials:

N-cyclopropyl-4-nitrobenzenesulfonamide

4-Nitrobenzenesulfonyl chloride

N,N-dicyclopropyl 4-nitrobenzenesulfonamide

Refernces