Technology Process of 10-[β-(2-phenylethylamino)ethylthio]dibenz[b,f]oxepin
There total 4 articles about 10-[β-(2-phenylethylamino)ethylthio]dibenz[b,f]oxepin which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: thionyl chloride / 0.17 h / Heating
2: 77 percent / AlCl3 / 1,2-dichloro-ethane / 2 h / Heating
3: boron trifluoride / acetic acid / 1.) RT, 16 h, 2.) reflux, 30 min
With
aluminium trichloride; thionyl chloride; boron trifluoride;
In
acetic acid; 1,2-dichloro-ethane;
DOI:10.1021/jm00179a005
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 88 percent / KOH / ethanol; H2O / 3 h / Heating
2: thionyl chloride / 0.17 h / Heating
3: 77 percent / AlCl3 / 1,2-dichloro-ethane / 2 h / Heating
4: boron trifluoride / acetic acid / 1.) RT, 16 h, 2.) reflux, 30 min
With
potassium hydroxide; aluminium trichloride; thionyl chloride; boron trifluoride;
In
ethanol; water; acetic acid; 1,2-dichloro-ethane;
DOI:10.1021/jm00179a005
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 77 percent / AlCl3 / 1,2-dichloro-ethane / 2 h / Heating
2: boron trifluoride / acetic acid / 1.) RT, 16 h, 2.) reflux, 30 min
With
aluminium trichloride; boron trifluoride;
In
acetic acid; 1,2-dichloro-ethane;
DOI:10.1021/jm00179a005
