C₃₀H₃₇N₇O₃S

Base Information

• Chemical Name: C₃₀H₃₇N₇O₃S
• CAS No.: 1562498-45-6
• Molecular Formula: C₃₀H₃₇N₇O₃S
• Molecular Weight: 575.735
• Mol file: 1562498-45-6.mol

Synonyms:

Chemical Property of C₃₀H₃₇N₇O₃S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₃₇N₇O₃S

There total 7 articles about C₃₀H₃₇N₇O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

C26H28N6O4S (1562498-36-5) + isobutylamine (78-81-9) → C30H37N7O3S (1562498-45-6)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; HATU; In dimethyl amine;

DOI:10.1016/j.bmcl.2013.12.123

Reference yield:

4-methoxybenzoic acid (100-09-4) → C30H37N7O3S (1562498-45-6)

Guidance literature:

Multi-step reaction with 7 steps

1.1: trichlorophosphate / acetonitrile / 1 h / 150 °C / Microwave irradiation

2.1: butan-1-ol / 3 h / 160 °C / Microwave irradiation

3.1: sodium hydrogencarbonate / water; dichloromethane

4.1: N,N-dimethyl-formamide / 4 h / 160 °C / Microwave irradiation

5.1: diammonium sulfide / N,N-dimethyl-formamide; methanol / 1 h / 100 °C / Microwave irradiation

5.2: 48 h / 23 °C / Microwave irradiation

6.1: ethanol / 1 h / 80 °C / Microwave irradiation

7.1: HATU; N-ethyl-N,N-diisopropylamine / dimethyl amine

With diammonium sulfide; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; HATU; trichlorophosphate; In methanol; ethanol; dichloromethane; water; dimethyl amine; N,N-dimethyl-formamide; acetonitrile; butan-1-ol; 6.1: |Hantzsch Thiazole Synthesis;

DOI:10.1016/j.bmcl.2013.12.123

Reference yield:

C13H9BrClN3O → C30H37N7O3S (1562498-45-6)

Guidance literature:

Multi-step reaction with 6 steps

1.1: butan-1-ol / 3 h / 160 °C / Microwave irradiation

2.1: sodium hydrogencarbonate / water; dichloromethane

3.1: N,N-dimethyl-formamide / 4 h / 160 °C / Microwave irradiation

4.1: diammonium sulfide / N,N-dimethyl-formamide; methanol / 1 h / 100 °C / Microwave irradiation

4.2: 48 h / 23 °C / Microwave irradiation

5.1: ethanol / 1 h / 80 °C / Microwave irradiation

6.1: HATU; N-ethyl-N,N-diisopropylamine / dimethyl amine

With diammonium sulfide; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; HATU; In methanol; ethanol; dichloromethane; water; dimethyl amine; N,N-dimethyl-formamide; butan-1-ol; 5.1: |Hantzsch Thiazole Synthesis;

DOI:10.1016/j.bmcl.2013.12.123

upstream raw materials:

C₂₆H₂₈N₆O₄S

isobutylamine

4-methoxybenzoic acid

C₂₃H₂₆N₆O₂

Refernces