Technology Process of C22H26ClN3O5S
There total 2 articles about C22H26ClN3O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
chlorotriisopropylsilane; trifluoroacetic acid;
In
dichloromethane;
at 22 ℃;
for 0.0833333h;
Inert atmosphere;
DOI:10.1021/ml300150y
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 3 h / 22 °C / Inert atmosphere
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 16 h / 22 °C / Inert atmosphere
3: pyridine / tetrahydrofuran; water; N,N-dimethyl-formamide / 3 h / 22 °C / Inert atmosphere
4: trifluoroacetic acid; chlorotriisopropylsilane / dichloromethane / 0.08 h / 22 °C / Inert atmosphere
With
pyridine; chlorotriisopropylsilane; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ml300150y
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; acetonitrile;
at 22 ℃;
for 70h;
Inert atmosphere;
DOI:10.1021/ml300150y