optically inactive 3-hydroxy-1.3-diphenyl-1-(fluorenyl-⁽⁹⁾)-propane

Base Information

• Chemical Name: optically inactive 3-hydroxy-1.3-diphenyl-1-(fluorenyl-⁽⁹⁾)-propane
• CAS No.: 859440-45-2
• Molecular Formula: C₂₈H₂₄O
• Molecular Weight: 376.498
• Mol file: 859440-45-2.mol

Synonyms:

Chemical Property of optically inactive 3-hydroxy-1.3-diphenyl-1-(fluorenyl-⁽⁹⁾)-propane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of optically inactive 3-hydroxy-1.3-diphenyl-1-(fluorenyl-⁽⁹⁾)-propane

There total 1 articles about optically inactive 3-hydroxy-1.3-diphenyl-1-(fluorenyl-⁽⁹⁾)-propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ optically inactive 3-hydroxy-1.3-diphenyl-1-(fluorenyl-(9))-propane (859440-45-2)

Guidance literature:

With aluminum isopropoxide; isopropyl alcohol;

DOI:10.1039/jr9490000050

Reference yield:

optically inactive 3-hydroxy-1.3-diphenyl-1-(fluorenyl-(9))-propane (859440-45-2) → 1,3-diphenyl-1,2,3,10b-tetrahydro-fluoranthene (859440-50-9)

Guidance literature:

With sulfuric acid; acetic acid; at 100 ℃;

DOI:10.1039/jr9490000050

Reference yield:

optically inactive 3-hydroxy-1.3-diphenyl-1-(fluorenyl-(9))-propane (859440-45-2) → 1,3-diphenyl-fluoranthene (71023-50-2)

Guidance literature:

Multi-step reaction with 2 steps

1: concentrated H₂SO₄; glacial acetic acid / 100 °C

2: palladium coal / 300 °C

With palladium on activated charcoal; sulfuric acid; acetic acid;

DOI:10.1039/jr9490000050

Downstream raw materials:

1,3-diphenyl-1,2,3,10b-tetrahydro-fluoranthene

1,3-diphenyl-fluoranthene