NH₂-SL-TGX

Base Information Edit

Chemical Name:NH₂-SL-TGX
CAS No.:1307865-00-4
Molecular Formula:C₃₂H₄₄N₆O₆
Molecular Weight:608.738
Hs Code.:
Mol file:1307865-00-4.mol

Synonyms:

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Chemical Property of NH₂-SL-TGX Edit

Chemical Property:

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Technology Process of NH₂-SL-TGX

There total 13 articles about NH₂-SL-TGX which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17282-00-7
3-bromo-5-methylpyridin-2-amine

: 1307865-00-4
NH₂-SL-TGX

Guidance literature:: Multi-step reaction with 11 steps

1.1: dichloromethane / 20 °C

2.1: methanesulfonyl chloride; triethylamine

3.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; N-ethyl-N,N-diisopropylamine

3.2: 20 °C

4.1: toluene / 4 h / Reflux; Molecular sieve; Inert atmosphere

5.1: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C

6.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 24 h / 85 °C

7.1: sodium tetrahydroborate; lithium chloride / tetrahydrofuran; ethanol / 24 h / 20 °C

8.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane

9.1: piperidine / dichloromethane

10.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane

11.1: trifluoroacetic acid / dichloromethane

With piperidine; dmap; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium tetrahydroborate; methanesulfonyl chloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; lithium chloride; In tetrahydrofuran; methanol; ethanol; dichloromethane; toluene; acetonitrile;
DOI:10.1021/mp200007b

Reference yield:

: 1307864-99-8
C₂₉H₃₉N₅O₄

: 1307865-00-4
NH₂-SL-TGX

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane

2: trifluoroacetic acid / dichloromethane

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/mp200007b

Reference yield:

: C₂₁H₂₂N₄O₂

: 1307865-00-4
NH₂-SL-TGX

Guidance literature:: Multi-step reaction with 7 steps

1: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C

2: N-ethyl-N,N-diisopropylamine / acetonitrile / 24 h / 85 °C

3: sodium tetrahydroborate; lithium chloride / tetrahydrofuran; ethanol / 24 h / 20 °C

4: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane

5: piperidine / dichloromethane

6: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane

7: trifluoroacetic acid / dichloromethane

With piperidine; dmap; sodium tetrahydroborate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; lithium chloride; In tetrahydrofuran; methanol; ethanol; dichloromethane; acetonitrile;
DOI:10.1021/mp200007b