Technology Process of C46H40N2O2S4
There total 5 articles about C46H40N2O2S4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ammonium acetate; acetic acid;
In
tetrahydrofuran;
for 20h;
Inert atmosphere;
Reflux;
DOI:10.1039/c1jm12181b
- Guidance literature:
-
Multi-step reaction with 2 steps
1: bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 4 h / Inert atmosphere; Reflux
2: ammonium acetate; acetic acid / tetrahydrofuran / 20 h / Inert atmosphere; Reflux
With
bis-triphenylphosphine-palladium(II) chloride; ammonium acetate; acetic acid;
In
tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c1jm12181b
- Guidance literature:
-
Multi-step reaction with 3 steps
1: N-Bromosuccinimide; acetic acid / chloroform / 1 h / Inert atmosphere; Reflux
2: bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 4 h / Inert atmosphere; Reflux
3: ammonium acetate; acetic acid / tetrahydrofuran / 20 h / Inert atmosphere; Reflux
With
bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; ammonium acetate; acetic acid;
In
tetrahydrofuran; chloroform; N,N-dimethyl-formamide;
DOI:10.1039/c1jm12181b