NH₂-Ala-Cys(H)-Cys(H)-Gly-OBzl

Base Information

• Chemical Name: NH₂-Ala-Cys(H)-Cys(H)-Gly-OBzl
• CAS No.: 114854-98-7
• Molecular Formula: C₁₈H₂₇N₅O₅S₂
• Molecular Weight: 457.575
• Mol file: 114854-98-7.mol

Synonyms:

Chemical Property of NH₂-Ala-Cys(H)-Cys(H)-Gly-OBzl

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of NH₂-Ala-Cys(H)-Cys(H)-Gly-OBzl

There total 2 articles about NH₂-Ala-Cys(H)-Cys(H)-Gly-OBzl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Z(OMe)-Cys(MBzl)-Gly-OBzl (114854-95-4) + Z(OMe)-Cys(Acm)(O)-Ala-NH2 → NH2-Ala-Cys(H)-Cys(H)-Gly-OBzl (114854-98-7)

Guidance literature:

With dimethylsulfide; In trifluoroacetic acid; at 25 ℃; for 2h;

DOI:10.1039/c39870001676

Reference yield:

Z(OMe)-Cys(Acm)(O)-Ala-NH2 + Z(OMe)-Cys(MBzl)-Gly-OBzl (114854-95-4) → NH2-Ala-Cys(H)-Cys(H)-Gly-OBzl (114854-98-7)

Guidance literature:

With trifluoroacetic acid; at 25 ℃; for 1h;

DOI:10.1016/S0040-4020(01)86118-4

upstream raw materials:

Z(OMe)-Cys(MBzl)-Gly-OBzl

Refernces

• 1、 Fujii, Nobutaka,Otaka, Akira,Watanabe, Toshihiro,Arai, Hiromitsu,Funakoshi, Susumu,et al.. "Sulphoxide-directed Disulphide Bond-forming Reaction for the Synthesis of Cystine Peptides". . p. 1676 - 1678. Retrieved 1987.