1-β-chloroethoxyperfluoro-2-methylcyclohexene

Base Information

• Chemical Name: 1-β-chloroethoxyperfluoro-2-methylcyclohexene
• CAS No.: 108431-83-0
• Molecular Formula: C₁₀H₄ClF₁₃O
• Molecular Weight: 422.573
• Mol file: 108431-83-0.mol

Synonyms:

Chemical Property of 1-β-chloroethoxyperfluoro-2-methylcyclohexene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-β-chloroethoxyperfluoro-2-methylcyclohexene

There total 1 articles about 1-β-chloroethoxyperfluoro-2-methylcyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.8%

perfluoro(1-ethylcyclohex-1-ene) (80308-96-9) + 2-chloro-ethanol (107-07-3) → 1-β-chloroethoxyperfluoro-2-methylcyclohexene (108431-83-0)

Guidance literature:

With triethylamine; at 0 ℃; for 1h;

DOI:10.1007/BF00956599

Reference yield:

1-β-chloroethoxyperfluoro-2-methylcyclohexene (108431-83-0) → cesium perfluoro-2-ethylcyclohexenol-1-ate

Guidance literature:

With cesium fluoride; In diethylene glycol dimethyl ether; at 120 ℃; for 6h;

DOI:10.1007/BF00956599

Reference yield:

1-β-chloroethoxyperfluoro-2-methylcyclohexene (108431-83-0) → perfluoro-2-ethylcyclohexen-3-one

Guidance literature:

Multi-step reaction with 2 steps

1: CsF / bis-(2-methoxy-ethyl) ether / 6 h / 120 °C

2: 150 °C / 10 Torr

With cesium fluoride; In diethylene glycol dimethyl ether;

DOI:10.1007/BF00956599

upstream raw materials:

perfluoro(1-ethylcyclohex-1-ene)

2-chloro-ethanol

Refernces