bis(triphenylphosphine)4-fluorobenzaldehyde thiosemicarbazone copper(I) acetate

Base Information

• Chemical Name: bis(triphenylphosphine)4-fluorobenzaldehyde thiosemicarbazone copper(I) acetate
• CAS No.: 952408-12-7
• Molecular Formula: C₂H₃O₂*C₄₄H₃₈CuFN₃P₂S
• Molecular Weight: 844.408
• Mol file: 952408-12-7.mol

Synonyms:

Chemical Property of bis(triphenylphosphine)4-fluorobenzaldehyde thiosemicarbazone copper(I) acetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of bis(triphenylphosphine)4-fluorobenzaldehyde thiosemicarbazone copper(I) acetate

There total 2 articles about bis(triphenylphosphine)4-fluorobenzaldehyde thiosemicarbazone copper(I) acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

Cu(I) bis(triphenylphosphine) acetate + (4-fluorobenzylidenehydrazinyl)thiocarboxamide (459-38-1) → bis(triphenylphosphine)4-fluorobenzaldehyde thiosemicarbazone copper(I) acetate (952408-12-7)

Guidance literature:

In methanol; to a stirred soln. of Cu-complex in methanol added an equimolar amts. ofthe organic ligand dissolved in methanol; stirred for 2 h at room temp.; soln. allowed to evaporate and a yellow product obtained; elem. anal.;

DOI:10.1016/j.poly.2007.04.026

Reference yield:

triphenylphosphine (603-35-0) → bis(triphenylphosphine)4-fluorobenzaldehyde thiosemicarbazone copper(I) acetate (952408-12-7)

Guidance literature:

Multi-step reaction with 2 steps

1: methanol

2: methanol

In methanol;

DOI:10.1016/j.poly.2007.04.026

upstream raw materials:

(4-fluorobenzylidenehydrazinyl)thiocarboxamide

triphenylphosphine

Refernces