C₅₅H₅₅N₁₃O₁₁S₆

Base Information

• Chemical Name: C₅₅H₅₅N₁₃O₁₁S₆
• CAS No.: 1344702-49-3
• Molecular Formula: C₅₅H₅₅N₁₃O₁₁S₆
• Molecular Weight: 1266.52
• Mol file: 1344702-49-3.mol

Synonyms:

Chemical Property of C₅₅H₅₅N₁₃O₁₁S₆

Chemical Property:

Purity/Quality:

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MSDS Files:

Useful:

Technology Process of C₅₅H₅₅N₁₃O₁₁S₆

There total 2 articles about C₅₅H₅₅N₁₃O₁₁S₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-acetoxybutyric acid (26976-72-7) → C55H55N13O11S6 (1344702-49-3)

Guidance literature:

Multi-step reaction with 2 steps

1: sulfuryl dichloride / dichloromethane / 16 h / 22 °C

2: pyridine / 0.25 h / 22 °C

With pyridine; sulfuryl dichloride; In dichloromethane;

DOI:10.1021/jm200938f

Reference yield:

C2HF3O2*C49H47N13O8S6 + 4-chloro-4-oxobutyl acetate (52762-35-3) → C55H55N13O11S6 (1344702-49-3)

Guidance literature:

With pyridine; at 22 ℃; for 0.25h;

DOI:10.1021/jm200938f

Reference yield: 5.0%

C55H55N13O11S6 (1344702-49-3) → C51H51N13O9S6 (960062-12-8)

Guidance literature:

With potassium carbonate; In methanol; for 2h;

DOI:10.1021/jm200938f

upstream raw materials:

4-chloro-4-oxobutyl acetate

4-acetoxybutyric acid

Downstream raw materials:

C₅₁H₅₁N₁₃O₉S₆

Refernces