4-Trifluoromethyl-2,3,5,6-tetrafluorophenyl prop-2-enyl ether

Base Information

• Chemical Name: 4-Trifluoromethyl-2,3,5,6-tetrafluorophenyl prop-2-enyl ether
• CAS No.: 349094-68-4
• Molecular Formula: C₁₀H₅F₇O
• Molecular Weight: 274.138
• Mol file: 349094-68-4.mol

Synonyms:

Chemical Property of 4-Trifluoromethyl-2,3,5,6-tetrafluorophenyl prop-2-enyl ether

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-Trifluoromethyl-2,3,5,6-tetrafluorophenyl prop-2-enyl ether

There total 1 articles about 4-Trifluoromethyl-2,3,5,6-tetrafluorophenyl prop-2-enyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

perfluorotoluene (434-64-0) + allyl alcohol (107-18-6) → 4-Trifluoromethyl-2,3,5,6-tetrafluorophenyl prop-2-enyl ether (349094-68-4)

Guidance literature:

With sodium allyloxide; for 0.7h; Heating;

DOI:10.1016/S0022-1139(00)00405-X

Reference yield: 21.0%

4-Trifluoromethyl-2,3,5,6-tetrafluorophenyl prop-2-enyl ether (349094-68-4) → 4-Trifluoromethyl-2,3,5,6-tetrafluorophenol (2787-79-3) + 2,3,5,6-Tetrafluoro-4-(prop-2-enyl)-4-(trifluoromethyl)-cyclohexa-2,5-dienone + 3-Trifluoromethyl-1,2,4,7-tetrafluorotricyclo[3.3.1.02,7]non-3-ene-8-one + 3-Trifluoromethyl-2,4,5,7-tetrafluorotricyclo[3.3.1.02,7]non-3-ene-6-one

Guidance literature:

at 350 ℃; Further byproducts given;

DOI:10.1016/S0022-1139(00)00405-X

upstream raw materials:

perfluorotoluene

allyl alcohol

Downstream raw materials:

4-Trifluoromethyl-2,3,5,6-tetrafluorophenol

Refernces