β-Dietilaminoetilestere dell'acido α-fluorofenilacetico

Base Information

• Chemical Name: β-Dietilaminoetilestere dell'acido α-fluorofenilacetico
• CAS No.: 22692-98-4
• Molecular Formula: C₁₄H₂₀FNO₂
• Molecular Weight: 253.317
• Mol file: 22692-98-4.mol

Synonyms:

Chemical Property of β-Dietilaminoetilestere dell'acido α-fluorofenilacetico

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of β-Dietilaminoetilestere dell'acido α-fluorofenilacetico

There total 4 articles about β-Dietilaminoetilestere dell'acido α-fluorofenilacetico which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bromo-phenyl-acetic acid methyl ester (37167-62-7,3042-81-7,61139-20-6) → β-Dietilaminoetilestere dell'acido α-fluorofenilacetico (22692-98-4)

Guidance literature:

Multi-step reaction with 4 steps

1: KF, AcNH₂ / 6 h / 120 °C

2: KOH / methanol

3: SOCl₂ / CHCl₃ / Heating

4: CHCl₃ / 15 h / Heating

With acetamide; potassium fluoride; potassium hydroxide; thionyl chloride; In methanol; chloroform;

Reference yield:

d'acide 2-fluoro-2-phenyl acetique (1578-63-8) → β-Dietilaminoetilestere dell'acido α-fluorofenilacetico (22692-98-4)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂ / CHCl₃ / Heating

2: CHCl₃ / 15 h / Heating

With thionyl chloride; In chloroform;

Reference yield:

methyl (±)-2-fluoro-2-phenylacetate (17841-30-4) → β-Dietilaminoetilestere dell'acido α-fluorofenilacetico (22692-98-4)

Guidance literature:

Multi-step reaction with 3 steps

1: KOH / methanol

2: SOCl₂ / CHCl₃ / Heating

3: CHCl₃ / 15 h / Heating

With potassium hydroxide; thionyl chloride; In methanol; chloroform;

upstream raw materials:

α-fluorophenylacetic acid chloride

2-(Diethylamino)ethanol

bromo-phenyl-acetic acid methyl ester

d'acide 2-fluoro-2-phenyl acetique

Refernces