phenacyl (R)-3-(octadecanoyloxy)octadecanoate

Base Information

• Chemical Name: phenacyl (R)-3-(octadecanoyloxy)octadecanoate
• CAS No.: 287922-82-1
• Molecular Formula: C₄₄H₇₆O₅
• Molecular Weight: 685.084
• Mol file: 287922-82-1.mol

Synonyms:

Chemical Property of phenacyl (R)-3-(octadecanoyloxy)octadecanoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of phenacyl (R)-3-(octadecanoyloxy)octadecanoate

There total 2 articles about phenacyl (R)-3-(octadecanoyloxy)octadecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

phenacyl (R)-3-hydroxyoctadecanoate (287922-81-0) + Stearoyl chloride (112-76-5) → phenacyl (R)-3-(octadecanoyloxy)octadecanoate (287922-82-1)

Guidance literature:

With pyridine; at 0 ℃; Inert atmosphere;

DOI:10.1002/chem.201003581

Reference yield:

(R)-β-hydroxyoctadecanoic acid methyl ester (2420-36-2,14531-40-9,14531-45-4,57793-27-8) → phenacyl (R)-3-(octadecanoyloxy)octadecanoate (287922-82-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: lithium hydroxide monohydrate / methanol; water / 20 °C

1.2: 20 °C

2.1: triethylamine / ethyl acetate / 0 - 20 °C / Inert atmosphere

3.1: pyridine / 0 °C / Inert atmosphere

With pyridine; lithium hydroxide monohydrate; triethylamine; In methanol; water; ethyl acetate;

DOI:10.1002/chem.201003581

upstream raw materials:

phenacyl (R)-3-hydroxyoctadecanoate

Stearoyl chloride

(R)-β-hydroxyoctadecanoic acid methyl ester

Refernces