CH3N(μ-BC6H5)(μ-CONCH3CO)NCH3

Base Information

• Chemical Name: CH3N(μ-BC6H5)(μ-CONCH3CO)NCH3
• CAS No.: 78594-57-7
• Molecular Formula: C₁₁H₁₄BN₃O₂
• Molecular Weight: 231.062
• Mol file: 78594-57-7.mol

Synonyms:

Chemical Property of CH3N(μ-BC6H5)(μ-CONCH3CO)NCH3

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of CH3N(μ-BC6H5)(μ-CONCH3CO)NCH3

There total 3 articles about CH3N(μ-BC6H5)(μ-CONCH3CO)NCH3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

1,3,5-trimethyl-biuret (816-00-2) + Bis-(dimethylamino)-phenylboran (1201-45-2) → CH3N(μ-BC6H5)(μ-CONCH3CO)NCH3 (78594-57-7)

Guidance literature:

In toluene; under Ar; refluxed for 7 h with stirring; filtd., the solvent is stripped under reduced pressure, the solid is sublimed under high vac., elem. anal.;

Reference yield: 71.0%

butyl-dichloro-borane (14090-22-3) + N,N',N''-Trimethyl-N,N''-bis(trimethylsilyl)biuret (10218-18-5) → CH3N(μ-BC6H5)(μ-CONCH3CO)NCH3 (78594-57-7)

Guidance literature:

In Petroleum ether; byproducts: (CH3)3SiCl; under N2, 4 h, reflux; the solvent and bromotrimethylsilane were removed in vac., the residue was distd.; elem. anal.;

Reference yield: 62.0%

N,N'-Dimethylurea (96-31-1) + 1,3,5-Trimethyl-2,4,6-triphenyl-borazin (909-21-7) → CH3N(μ-BC6H5)(μ-CONCH3CO)NCH3 (78594-57-7)

Guidance literature:

In neat (no solvent); mixt. carefully melted, boiled (10 min), cooled to room temp., addn. of benzene, refluxed (stirring, 15 min), decanted (clear soln.); evapn., unreacted urea sublimed off (under vacuum, 80°C bath temp.), residiue dissolved (benzene, insol. material discarded), evapn., sublimed (under vacuum);

upstream raw materials:

butyl-dichloro-borane

N,N',N''-Trimethyl-N,N''-bis(trimethylsilyl)biuret

N,N'-Dimethylurea

1,3,5-Trimethyl-2,4,6-triphenyl-borazin

Refernces

• 1、 Maringgele, Walter. "Reaction of Metal and Metalloid Compounds with Polyfunctional Molecules, XXXVI. New Syntheses of Open-Chain and Cyclic N-Borylureas and -thioureas". . p. 3271 - 3289. Retrieved 2007/10/02.