C₂₆H₂₈N₆O₄S

Base Information

• Chemical Name: C₂₆H₂₈N₆O₄S
• CAS No.: 1562498-36-5
• Molecular Formula: C₂₆H₂₈N₆O₄S
• Molecular Weight: 520.612
• Mol file: 1562498-36-5.mol

Synonyms:

Chemical Property of C₂₆H₂₈N₆O₄S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₂₈N₆O₄S

There total 7 articles about C₂₆H₂₈N₆O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

bromopyruvic acid (1113-59-3) + C23H28N6O2S (1562498-31-0) → C26H28N6O4S (1562498-36-5)

Guidance literature:

In ethanol; at 80 ℃; for 1h; Microwave irradiation;

DOI:10.1016/j.bmcl.2013.12.123

Reference yield:

4-methoxybenzoic acid (100-09-4) → C26H28N6O4S (1562498-36-5)

Guidance literature:

Multi-step reaction with 6 steps

1.1: trichlorophosphate / acetonitrile / 1 h / 150 °C / Microwave irradiation

2.1: butan-1-ol / 3 h / 160 °C / Microwave irradiation

3.1: sodium hydrogencarbonate / water; dichloromethane

4.1: N,N-dimethyl-formamide / 4 h / 160 °C / Microwave irradiation

5.1: diammonium sulfide / N,N-dimethyl-formamide; methanol / 1 h / 100 °C / Microwave irradiation

5.2: 48 h / 23 °C / Microwave irradiation

6.1: ethanol / 1 h / 80 °C / Microwave irradiation

With diammonium sulfide; sodium hydrogencarbonate; trichlorophosphate; In methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; butan-1-ol; 6.1: |Hantzsch Thiazole Synthesis;

DOI:10.1016/j.bmcl.2013.12.123

Reference yield:

C23H26N6O2 (1591733-54-8) → C26H28N6O4S (1562498-36-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: diammonium sulfide / N,N-dimethyl-formamide; methanol / 1 h / 100 °C / Microwave irradiation

1.2: 48 h / 23 °C / Microwave irradiation

2.1: ethanol / 1 h / 80 °C / Microwave irradiation

With diammonium sulfide; In methanol; ethanol; N,N-dimethyl-formamide; 2.1: |Hantzsch Thiazole Synthesis;

DOI:10.1016/j.bmcl.2013.12.123

upstream raw materials:

bromopyruvic acid

C₂₃H₂₈N₆O₂S

4-methoxybenzoic acid

C₂₃H₂₆N₆O₂

Downstream raw materials:

C₂₆H₂₉N₇O₃S

C₃₀H₃₇N₇O₃S

Refernces