Technology Process of ethyl 5-chloro-2,4-dihydroxy-6-propylbenzoate
There total 1 articles about ethyl 5-chloro-2,4-dihydroxy-6-propylbenzoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sulfuryl dichloride;
In
diethyl ether;
for 2h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) 15percent aq. NaOH, 2.) conc. HCl / 1.) reflux, 3 h, 2.) reflux, 10 min
2: K2CO3 / acetone / 10 h
With
hydrogenchloride; sodium hydroxide; potassium carbonate;
In
acetone;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) 15percent aq. NaOH, 2.) conc. HCl / 1.) reflux, 3 h, 2.) reflux, 10 min
2: K2CO3 / acetone / 10 h
3: 83 percent / I2, HgO / diethyl ether / 24 h / Ambient temperature
With
hydrogenchloride; sodium hydroxide; iodine; potassium carbonate; mercury(II) oxide;
In
diethyl ether; acetone;
