C₁₅H₁₅NS

Base Information

• Chemical Name: C₁₅H₁₅NS
• CAS No.: 177265-17-7
• Molecular Formula: C₁₅H₁₅NS
• Molecular Weight: 241.357
• Mol file: 177265-17-7.mol

Synonyms:

Chemical Property of C₁₅H₁₅NS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₁₅NS

There total 1 articles about C₁₅H₁₅NS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

di(p-tolyl) disulfide (103-19-5) + acetophenone (98-86-2) → C15H15NS (177265-17-7)

Guidance literature:

With ammonia; silver nitrate; Yield given. Multistep reaction; 1.) MeOH, 0 deg C, 15 min, 2.) r.t., 16 h;

DOI:10.1039/p19960000691

Reference yield: 50.0%

C15H15NS (177265-17-7) → (+/-)-(S,E)-N-(1-Phenylethylidene)toluene-p-sulfinamide (81801-27-6)

Guidance literature:

With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In chloroform; 1.) 0 deg C, 30 min, 2.) r.t., 30 min;

DOI:10.1039/p19960000691

Reference yield:

C15H15NS (177265-17-7) → 4-Methyl-benzenesulfinic acid [1-phenyl-eth-(E)-ylidene]-amide (188447-75-8)

Guidance literature:

With (-)-N-(phenylsulfonyl)-(3,3-dichlorocamphoryl)oxaziridine; In tetrachloromethane; for 48h; Yield given;

DOI:10.1021/jo00050a007

upstream raw materials:

di(p-tolyl) disulfide

acetophenone

Downstream raw materials:

4-Methyl-benzenesulfinic acid [1-phenyl-eth-(E)-ylidene]-amide

(+/-)-(S,E)-N-(1-Phenylethylidene)toluene-p-sulfinamide

[S-(E)]-(+)-N-α-methylbenzylidene-p-toluenesulfinamide

(R,S_S)-N-α-methylbenzyl-p-tolylsulfinamide

Refernces