CH₃Cu(PPh₃)3*THF

Base Information

• Chemical Name: CH₃Cu(PPh₃)3*THF
• CAS No.: 123074-76-0
• Molecular Formula: C₄H₈O*C₅₅H₄₈CuP₃
• Molecular Weight: 937.56
• Mol file: 123074-76-0.mol

Synonyms:

Chemical Property of CH₃Cu(PPh₃)3*THF

Chemical Property:

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Technology Process of CH₃Cu(PPh₃)3*THF

There total 1 articles about CH₃Cu(PPh₃)3*THF which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

copper diacetate (142-71-2) + aluminium dimethylisopropoxide (6063-89-4) → CH3Cu(PPh3)3*THF (123074-76-0)

Guidance literature:

With P(C₆H₅)3; C₄H₈O; In diethyl ether; Schlenk flask cooled to -78°C, after addn. of educts slowly warming of the flask to -25°C, cooling of the soln. to -100°C,; filtration, recrystn. at -15°C from THF/pentane;

DOI:10.1021/om00113a032

upstream raw materials:

copper diacetate

aluminium dimethylisopropoxide

Refernces