7,12-bis(benzoyloxy)heptacyclo<6.6.0.0^2,6.0^3,13.0^4,11.0^5,9.0^10,14>tetradecane

Base Information

• Chemical Name: 7,12-bis(benzoyloxy)heptacyclo<6.6.0.0^2,6.0^3,13.0^4,11.0^5,9.0^10,14>tetradecane
• CAS No.: 89278-39-7
• Molecular Formula: C₂₈H₂₄O₄
• Molecular Weight: 424.496
• Mol file: 89278-39-7.mol

Synonyms:

Chemical Property of 7,12-bis(benzoyloxy)heptacyclo<6.6.0.0^2,6.0^3,13.0^4,11.0^5,9.0^10,14>tetradecane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 7,12-bis(benzoyloxy)heptacyclo<6.6.0.0^2,6.0^3,13.0^4,11.0^5,9.0^10,14>tetradecane

There total 5 articles about 7,12-bis(benzoyloxy)heptacyclo<6.6.0.0^2,6.0^3,13.0^4,11.0^5,9.0^10,14>tetradecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

7-benzoyloxynorbornadiene (4796-68-3) → 7,12-bis(benzoyloxy)heptacyclo<6.6.0.02,6.03,13.04,11.05,9.010,14>tetradecane (89278-39-7) + C29H24O5 (104351-89-5) + C29H24O5 (104419-67-2) + C29H24O5 (104351-88-4)

Guidance literature:

In dibutyl ether; for 72h; Further byproducts given; Heating;

DOI:10.1021/jo00372a002

Reference yield: 29.0%

7-benzoyloxynorbornadiene (4796-68-3) → 7,12-bis(benzoyloxy)heptacyclo<6.6.0.02,6.03,13.04,11.05,9.010,14>tetradecane (89278-39-7) + C29H24O5 (104419-67-2) + C29H24O5 (104351-88-4) + C29H24O5 (104419-68-3)

Guidance literature:

In dibutyl ether; for 72h; Further byproducts given; Heating;

DOI:10.1021/jo00372a002

Reference yield: 29.0%

7-benzoyloxynorbornadiene (4796-68-3) → 7,12-bis(benzoyloxy)heptacyclo<6.6.0.02,6.03,13.04,11.05,9.010,14>tetradecane (89278-39-7) + C29H24O5 (104351-89-5) + C29H24O5 (104419-67-2) + C29H24O5 (104351-88-4) + C29H24O5 (104419-68-3)

Guidance literature:

With iron pentacarbonyl; In dibutyl ether; for 72h; Mechanism; Product distribution; Heating; 7-<(p-methoxybenzoyl)oxy>norbornadiene;

DOI:10.1021/jo00372a002

upstream raw materials:

7-benzoyloxynorbornadiene

Refernces

• 1、 Marchand, Alan P.,Earlywine, Arthur D.. "-". . p. 1660 - 1661. Retrieved 2007/10/02.