C₂₄H₂₆N₂O₃

Base Information

• Chemical Name: C₂₄H₂₆N₂O₃
• CAS No.: 409312-96-5
• Molecular Formula: C₂₄H₂₆N₂O₃
• Molecular Weight: 390.482
• Mol file: 409312-96-5.mol

Synonyms:

Chemical Property of C₂₄H₂₆N₂O₃

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

4,6-Bis((S)-4-isopropyl-4,5-dihydrooxazol-2-yl)dibenzo[b,d]furan 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₂₆N₂O₃

There total 3 articles about C₂₄H₂₆N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R)-2-amino-3-methylbutanol (4276-09-9,473-75-6) + dibenzofuran-4,6-dicarbonyl chloride (51412-73-8) → C24H26N2O3 (409312-96-5)

Guidance literature:

With sodium hydroxide; thionyl chloride; triethylamine; Multistep reaction;

DOI:10.1021/ja973519c

Reference yield:

dibenzofuran (132-64-9,214827-48-2) → C24H26N2O3 (409312-96-5)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) BuLi / 1.) THF, hexane, from -40 deg C to reflux, 4,5 h, 2.) THF, hexane

2: SOCl₂, CF₃COOH / 13 h / Heating

3: 1.) Et₃N, 2.) SOCl₂, 3.) aq. NaOH

With sodium hydroxide; n-butyllithium; thionyl chloride; triethylamine; trifluoroacetic acid;

DOI:10.1021/ja973519c

Reference yield:

dibenzofuran-4,6-dicarboxylic acid (88818-47-7) → C24H26N2O3 (409312-96-5)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂, CF₃COOH / 13 h / Heating

2: 1.) Et₃N, 2.) SOCl₂, 3.) aq. NaOH

With sodium hydroxide; thionyl chloride; triethylamine; trifluoroacetic acid;

DOI:10.1021/ja973519c

upstream raw materials:

(R)-2-amino-3-methylbutanol

dibenzofuran-4,6-dicarbonyl chloride

dibenzofuran

dibenzofuran-4,6-dicarboxylic acid

Refernces