Mesoxalylchlorid-2-benzyloxyphenylhydrazon

Base Information

• Chemical Name: Mesoxalylchlorid-2-benzyloxyphenylhydrazon
• CAS No.: 92854-24-5
• Molecular Formula: C₁₆H₁₂Cl₂N₂O₃
• Molecular Weight: 351.189
• Mol file: 92854-24-5.mol

Synonyms:

Chemical Property of Mesoxalylchlorid-2-benzyloxyphenylhydrazon

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Mesoxalylchlorid-2-benzyloxyphenylhydrazon

There total 3 articles about Mesoxalylchlorid-2-benzyloxyphenylhydrazon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-benzyloxynitrobenzene (4560-41-2) → Mesoxalylchlorid-2-benzyloxyphenylhydrazon (92854-24-5)

Guidance literature:

Multi-step reaction with 4 steps

1: H₂ / Adams catalyst

2: (i) aq. HCl, (ii) NaNO₂, (iii) /BRN= 774687/, aq. NaOAc

3: aq. NaOH

4: SOCl₂

With sodium hydroxide; thionyl chloride; hydrogen; platinum(IV) oxide;

DOI:10.1039/jr9610002828

Reference yield:

Mesoxalsaeure-2-benzyloxyphenylhydrazon (93014-48-3) → Mesoxalylchlorid-2-benzyloxyphenylhydrazon (92854-24-5)

Guidance literature:

With thionyl chloride;

DOI:10.1039/jr9610002828

Reference yield:

Diethylmesoxalat-2-benzyloxyphenylhydrazon (94680-63-4) → Mesoxalylchlorid-2-benzyloxyphenylhydrazon (92854-24-5)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. NaOH

2: SOCl₂

With sodium hydroxide; thionyl chloride;

DOI:10.1039/jr9610002828

upstream raw materials:

Mesoxalsaeure-2-benzyloxyphenylhydrazon

2-benzyloxynitrobenzene

Diethylmesoxalat-2-benzyloxyphenylhydrazon