Stearoylpiperidide

Base Information

• Chemical Name: Stearoylpiperidide
• CAS No.: 4629-04-3
• Molecular Formula: C₂₃H₄₅NO
• Molecular Weight: 351.616
• Mol file: 4629-04-3.mol

Synonyms:

Chemical Property of Stearoylpiperidide

Chemical Property:

• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

99% ^*data from raw suppliers

1-(Piperidin-1-yl)octadecan-1-one 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Stearoylpiperidide

There total 6 articles about Stearoylpiperidide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

piperidine (110-89-4) + stearic acid (57-11-4) → 1-(piperidin-1-yl)octadecan-1-one (4629-04-3)

Guidance literature:

stearic acid; With 4-methyl-morpholine; In tetrahydrofuran; for 3h;

piperidine; With 4-methyl-morpholine; In tetrahydrofuran; for 3h; Further stages.;

DOI:10.1021/ol990215h

Reference yield: 58.0%

piperidine (110-89-4) + distearoyl diselenide (65212-12-6) → 1-(piperidin-1-yl)octadecan-1-one (4629-04-3) + Octadecaneselenoic acid; compound with piperidine (105223-36-7)

Guidance literature:

In dichloromethane; at 5 ℃; for 0.333333h;

DOI:10.1055/s-1986-31494

Reference yield:

N-piperidyl-9-octadecenamide (56630-42-3) → 1-(piperidin-1-yl)octadecan-1-one (4629-04-3)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol;

upstream raw materials:

piperidine

Stearoyl chloride

distearoyl diselenide

1,5-Dioctadecanoyl-[1,3,5]triazinane-2,4-dione

Downstream raw materials:

1-(4-dimethylamino-phenyl)-octadecan-1-one

Refernces

• 1、 Hosseini-Sarvari, Mona,Sodagar, Esmat,Doroodmand, Mohammad Mahdi. "Nano sulfated titania as solid acid catalyst in direct synthesis of fatty acid amides". supporting information; experimental part. p. 2853 - 2859. Retrieved 2011/05/17.
• 2、 Masala, Simonetta,Taddei, Maurizio. "Solid-supported chloro[1,3,5]triazine. A versatile new synthetic auxiliary for the synthesis of amide libraries". . p. 1355 - 1357. Retrieved 2008/02/09.