2,3-Dihydroxy-cyclohexancarbonsaeuremethylester

Base Information

• Chemical Name: 2,3-Dihydroxy-cyclohexancarbonsaeuremethylester
• CAS No.: 72842-19-4
• Molecular Formula: C₈H₁₄O₄
• Molecular Weight: 174.197
• Mol file: 72842-19-4.mol

Synonyms:

Chemical Property of 2,3-Dihydroxy-cyclohexancarbonsaeuremethylester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3-Dihydroxy-cyclohexancarbonsaeuremethylester

There total 4 articles about 2,3-Dihydroxy-cyclohexancarbonsaeuremethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl-2,3-dihydroxybenzoate (2411-83-8) → 2,3-Dihydroxy-cyclohexancarbonsaeuremethylester (72842-19-4)

Guidance literature:

With hydrogen; rhodium on alumina; under 3102.9 Torr;

DOI:10.1002/jps.2600680915

Reference yield:

2,3-dimethoxybenzoic acid (1521-38-6) → 2,3-Dihydroxy-cyclohexancarbonsaeuremethylester (72842-19-4)

Guidance literature:

Multi-step reaction with 3 steps

1: HCl, H₂SO₄

2: BCl₃

3: H₂ / Rh-Al₂O₃ / 3102.9 Torr

With hydrogenchloride; sulfuric acid; hydrogen; boron trichloride; rhodium on alumina;

DOI:10.1002/jps.2600680915

Reference yield:

methyl 2,3-dimethoxybenzoate (2150-42-7) → 2,3-Dihydroxy-cyclohexancarbonsaeuremethylester (72842-19-4)

Guidance literature:

Multi-step reaction with 2 steps

1: BCl₃

2: H₂ / Rh-Al₂O₃ / 3102.9 Torr

With hydrogen; boron trichloride; rhodium on alumina;

DOI:10.1002/jps.2600680915

upstream raw materials:

methyl-2,3-dihydroxybenzoate

2,3-dimethoxybenzoic acid

methyl 2,3-dimethoxybenzoate

2,3-dimethyoxybenzaldehyde

Downstream raw materials:

3-Acetoxy-Δ¹-cyclohexencarbonsaeuremethylester

Refernces