Technology Process of Fmoc-Gln(Trt)-ODhbt
There total 5 articles about Fmoc-Gln(Trt)-ODhbt which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 35 percent / Ac2O, conc.H2SO4 / acetic acid / 60 °C
3: DCC / tetrahydrofuran / or in EtOAc
With
sulfuric acid; acetic anhydride; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; acetic acid;
DOI:10.1016/S0040-4039(00)74872-6
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 93 percent / H2, 1N HCl / 10percent Pd-C / methanol; H2O / 1 h
3: DCC / tetrahydrofuran / or in EtOAc
With
hydrogenchloride; hydrogen; dicyclohexyl-carbodiimide;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; water;
DOI:10.1016/S0040-4039(00)74872-6
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 35 percent / Ac2O, conc.H2SO4 / acetic acid / 60 °C
3: DCC / tetrahydrofuran / or in EtOAc
With
sulfuric acid; acetic anhydride; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; acetic acid;
DOI:10.1016/S0040-4039(00)74872-6