Technology Process of α-Brom-N-tosyl-2-<4-(trimethylsilyl)phenyl>-acetohydrazonoylchlorid
There total 5 articles about α-Brom-N-tosyl-2-<4-(trimethylsilyl)phenyl>-acetohydrazonoylchlorid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
phenol;
In
dichloromethane;
for 0.5h;
Yield given;
Heating;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: NBS, azobis(isobutyronitrile) / CCl4 / Heating
2: 63 percent / CH2Cl2 / 0.5 h
3: PCl5 / CH2Cl2 / 1.) room temp.; 2.) 30 min, reflux
4: phenol / CH2Cl2 / 0.5 h / Heating
With
N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); phosphorus pentachloride; phenol;
In
tetrachloromethane; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: SOCl2 / CCl4 / 1.) slowly to 65 deg C; 2.) 30 min, reflux
2: NBS, azobis(isobutyronitrile) / CCl4 / Heating
3: 63 percent / CH2Cl2 / 0.5 h
4: PCl5 / CH2Cl2 / 1.) room temp.; 2.) 30 min, reflux
5: phenol / CH2Cl2 / 0.5 h / Heating
With
N-Bromosuccinimide; thionyl chloride; 2,2'-azobis(isobutyronitrile); phosphorus pentachloride; phenol;
In
tetrachloromethane; dichloromethane;
