Technology Process of C11H21NO5
There total 5 articles about C11H21NO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
4-methyl-morpholine; osmium(VIII) oxide;
In
acetone;
at 20 ℃;
for 15h;
DOI:10.1002/chem.201402175
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate; methanol / 4 h / 20 °C
2: 4-methyl-morpholine; osmium(VIII) oxide / acetone / 15 h / 20 °C
With
4-methyl-morpholine; methanol; osmium(VIII) oxide; potassium carbonate;
In
acetone;
DOI:10.1002/chem.201402175
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: bis(η3-allyl-μ-chloropalladium(II)); trans-1,2-(1S,2S)-1,2-diaminocyclohexane-N,N’-bis(2’-diphenylphosphinobenzoyl) / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere
1.2: 1.5 h / 0 °C / Inert atmosphere
2.1: water; trimethylphosphane / tetrahydrofuran / 2 h / Inert atmosphere
3.1: triethylamine / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere
4.1: potassium carbonate; methanol / 4 h / 20 °C
5.1: 4-methyl-morpholine; osmium(VIII) oxide / acetone / 15 h / 20 °C
With
4-methyl-morpholine; methanol; trans-1,2-(1S,2S)-1,2-diaminocyclohexane-N,N’-bis(2’-diphenylphosphinobenzoyl); osmium(VIII) oxide; bis(η3-allyl-μ-chloropalladium(II)); water; potassium carbonate; triethylamine; trimethylphosphane;
In
tetrahydrofuran; acetone;
2.1: |Staudinger Azide Reduction;
DOI:10.1002/chem.201402175
