Technology Process of 2-(2,4-dichlorobenzyloxy)-N-phthaloylethylamine
There total 2 articles about 2-(2,4-dichlorobenzyloxy)-N-phthaloylethylamine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 91 percent / NaOH / 1 h / 80 °C
2: 84 percent / SOCl2 / 1,2-dichloro-ethane / 1.5 h / Heating
3: 80 percent / dimethylformamide / 115 - 120 °C
With
sodium hydroxide; thionyl chloride;
In
1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1007/BF00772012
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 84 percent / SOCl2 / 1,2-dichloro-ethane / 1.5 h / Heating
2: 80 percent / dimethylformamide / 115 - 120 °C
With
thionyl chloride;
In
1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1007/BF00772012
- Guidance literature:
-
With
hydrazine hydrate;
In
ethanol;
for 0.5h;
Heating;
DOI:10.1007/BF00772012
