dicarbonyl(2,4-dimethoxybenzoato)hydridobis(triethylphosphino)iron

Base Information

• Chemical Name: dicarbonyl(2,4-dimethoxybenzoato)hydridobis(triethylphosphino)iron
• CAS No.: 131011-76-2
• Molecular Formula: C₂₃H₄₀FeO₆P₂
• Molecular Weight: 530.362
• Mol file: 131011-76-2.mol

Synonyms:

Chemical Property of dicarbonyl(2,4-dimethoxybenzoato)hydridobis(triethylphosphino)iron

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of dicarbonyl(2,4-dimethoxybenzoato)hydridobis(triethylphosphino)iron

There total 1 articles about dicarbonyl(2,4-dimethoxybenzoato)hydridobis(triethylphosphino)iron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

μ-dinitrogenbis{dicarbonylbis(triethylphosphane)-iron} (107654-09-1) + 2,4 dimethoxybenzoic acid (91-52-1) → dicarbonyl(2,4-dimethoxybenzoato)hydridobis(triethylphosphino)iron (131011-76-2)

Guidance literature:

With Na₂CO₃; In diethyl ether; byproducts: N2; (N2); -70°C; slowly warming; pouring onto Na2CO3; stirring for 15 min; filtration (silica gel); removal of solvent in vac.; chromy.; removal of solvent from yellow eluate in vac.; dissolving in hexan; crystn. at -30°C; elem.anal.;

upstream raw materials:

μ-dinitrogenbis{dicarbonylbis(triethylphosphane)-iron}

2,4 dimethoxybenzoic acid

Refernces