Technology Process of C43H76NO9P
There total 5 articles about C43H76NO9P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 94 percent / pyridine; CH2Cl2 / Ambient temperature
2: H2 / 10percent Pd-C / butan-2-one / 3 h / 760 Torr / Ambient temperature
3: N,N-dimethylaminopyridine / CH2Cl2 / 24 h / Ambient temperature
4: Zn/CH3COOH / diethyl ether / 0.5 h / Ambient temperature
5: 1.) (C2H5)3N, N,N-dimethylaminopyridine / 1.) benzene, room temp., overnight, 2.) CH3CN, 60 deg C, 5 h
With
dmap; hydrogen; acetic acid; triethylamine; zinc;
palladium on activated charcoal;
In
pyridine; diethyl ether; dichloromethane; butanone;
DOI:10.1055/s-1987-27845
- Guidance literature:
-
Multi-step reaction with 4 steps
1: H2 / 10percent Pd-C / butan-2-one / 3 h / 760 Torr / Ambient temperature
2: N,N-dimethylaminopyridine / CH2Cl2 / 24 h / Ambient temperature
3: Zn/CH3COOH / diethyl ether / 0.5 h / Ambient temperature
4: 1.) (C2H5)3N, N,N-dimethylaminopyridine / 1.) benzene, room temp., overnight, 2.) CH3CN, 60 deg C, 5 h
With
dmap; hydrogen; acetic acid; triethylamine; zinc;
palladium on activated charcoal;
In
diethyl ether; dichloromethane; butanone;
DOI:10.1055/s-1987-27845
- Guidance literature:
-
Multi-step reaction with 3 steps
1: N,N-dimethylaminopyridine / CH2Cl2 / 24 h / Ambient temperature
2: Zn/CH3COOH / diethyl ether / 0.5 h / Ambient temperature
3: 1.) (C2H5)3N, N,N-dimethylaminopyridine / 1.) benzene, room temp., overnight, 2.) CH3CN, 60 deg C, 5 h
With
dmap; acetic acid; triethylamine; zinc;
In
diethyl ether; dichloromethane;
DOI:10.1055/s-1987-27845
