Technology Process of C21H20Cl2N6O3
There total 12 articles about C21H20Cl2N6O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
organic base;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 2h;
DOI:10.1021/jf102842r
- Guidance literature:
-
Multi-step reaction with 7 steps
1: dichloromethane
2: pyridine / 1 h / 20 °C
3: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C
4: organic base / dichloromethane / 0 - 20 °C
5: sodium azide / water; acetone / 20 h / 20 °C
6: palladium 10% on activated carbon; hydrogen / methanol / 4 h / 25 °C
7: organic base / tetrahydrofuran / 2 h / 0 - 20 °C
With
pyridine; lithium aluminium tetrahydride; sodium azide; palladium 10% on activated carbon; hydrogen;
In
tetrahydrofuran; methanol; dichloromethane; water; acetone;
DOI:10.1021/jf102842r
- Guidance literature:
-
Multi-step reaction with 6 steps
1: pyridine / 1 h / 20 °C
2: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C
3: organic base / dichloromethane / 0 - 20 °C
4: sodium azide / water; acetone / 20 h / 20 °C
5: palladium 10% on activated carbon; hydrogen / methanol / 4 h / 25 °C
6: organic base / tetrahydrofuran / 2 h / 0 - 20 °C
With
pyridine; lithium aluminium tetrahydride; sodium azide; palladium 10% on activated carbon; hydrogen;
In
tetrahydrofuran; methanol; dichloromethane; water; acetone;
DOI:10.1021/jf102842r
