Hydrazine Dicarbonic Acid Diazide

Base Information

• Chemical Name: Hydrazine Dicarbonic Acid Diazide
• CAS No.: 67880-17-5
• Molecular Formula: C2H2 N8 O2
• Molecular Weight: 170.09
• DSSTox Substance ID: DTXSID001308015
• Nikkaji Number: J59.881J
• Mol file: 67880-17-5.mol

Synonyms:Hydrazine Dicarbonic Acid Diazide;67880-17-5;Hydrazine dicarbonic acid diazide [Forbidden];1,2-Hydrazinedicarbonyl azide;DTXSID001308015

Chemical Property of Hydrazine Dicarbonic Acid Diazide

Chemical Property:

• Refractive Index: 1.6910 (estimate)
• Boiling Point: 299.69°C (rough estimate)
• PSA: 157.70000
• LogP: 0.62852
• XLogP3: 1.8
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 0
• Exact Mass: 170.03007134
• Heavy Atom Count: 12
• Complexity: 251

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(=O)(NNC(=O)N=[N+]=[N-])N=[N+]=[N-]

Technology Process of Hydrazine Dicarbonic Acid Diazide

There total 3 articles about Hydrazine Dicarbonic Acid Diazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

N,N'-bis(hydrazocarbonyl) hydrazide (1617-13-6) → Hydrazodicarbonazid (germ.)=hydrazodicarbonic azide (67880-17-5)

Guidance literature:

With hydrogenchloride; acetic acid; sodium nitrite; at -5 ℃; for 0.25h;

Reference yield:

carbonodihydrazide (497-18-7) → carbonyl azide (14435-92-8) + Hydrazodicarbonazid (germ.)=hydrazodicarbonic azide (67880-17-5)

Guidance literature:

With water; Petroleum ether; Diazotization;

Reference yield:

→ Hydrazodicarbonazid (germ.)=hydrazodicarbonic azide (67880-17-5)

Guidance literature:

With water; sodium nitrite;

upstream raw materials:

carbonodihydrazide

N,N'-bis(hydrazocarbonyl) hydrazide

Downstream raw materials:

hydrogen azide

hydrazine

diethyl hydrazinedicarboxylate

1-phenylcarbamoyl-4-phenyl semicarbazide

Refernces

• 1、 Harris, Joanna M.,McDonald, Robert,Vederas, John C.. "Synthesis of a chiral azodicarboxamide containing a bridging binaphthyl moiety: electrophilic amination reactions of achiral ester enolates". . p. 2669 - 2674. Retrieved 2007/10/03.