Bis-(5-methyl-furan-2-yl)-methanone

Base Information

• Chemical Name: Bis-(5-methyl-furan-2-yl)-methanone
• CAS No.: 21432-51-9
• Molecular Formula: C₁₁H₁₀O₃
• Molecular Weight: 190.199
• Mol file: 21432-51-9.mol

Synonyms:

Chemical Property of Bis-(5-methyl-furan-2-yl)-methanone

Chemical Property:

• Melting Point: 192-197 °C
• Boiling Point: 308.1±42.0 °C(Predicted)
• Density: 1.147±0.06 g/cm3(Predicted)

Purity/Quality:

98% ^*data from raw suppliers

Bis-(5-methyl-furan-2-yl)-methanone ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Bis-(5-methyl-furan-2-yl)-methanone

There total 2 articles about Bis-(5-methyl-furan-2-yl)-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

2',2-methylenebis-(5-methylfuran) (13679-43-1) → bis(5-methylfuran-2-yl)methanone (21432-51-9)

Guidance literature:

With potassium permanganate; In acetonitrile; at 20 ℃; for 3.25h;

Reference yield:

2-methylfuran (534-22-5) → bis(5-methylfuran-2-yl)methanone (21432-51-9)

Guidance literature:

Multi-step reaction with 2 steps

1: sulfuric acid / methanol; water / 24 h / 0 - 20 °C / Sealed tube

2: potassium permanganate / acetonitrile / 3.25 h / 20 °C

With potassium permanganate; sulfuric acid; In methanol; water; acetonitrile;

upstream raw materials:

2',2-methylenebis-(5-methylfuran)

2-methylfuran

Refernces