tetraphenylantimony 4-hydroxybenzenesulfonate

Base Information

• Chemical Name: tetraphenylantimony 4-hydroxybenzenesulfonate
• CAS No.: 209463-67-2
• Molecular Formula: C₆H₅O₄S*C₂₄H₂₀Sb
• Molecular Weight: 603.342
• Mol file: 209463-67-2.mol

Synonyms:

Chemical Property of tetraphenylantimony 4-hydroxybenzenesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tetraphenylantimony 4-hydroxybenzenesulfonate

There total 2 articles about tetraphenylantimony 4-hydroxybenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

p-hydoroxybenzenesulfonic acid (98-67-9) + pentaphenylantimony (2170-05-0) → tetraphenylantimony 4-hydroxybenzenesulfonate (209463-67-2)

Guidance literature:

In benzene; mixt. of 4-sulfophenol and BiPh5 in C6H6 kept at 20°C for 0.5 h; solvent removed, washed (hexane), dried; elem. anal.;

DOI:10.1134/S1070328407030037

Reference yield: 87.0%

triphenylantimonybismuth bis(4-hydroxybenzenesulfonate) + pentaphenylantimony (2170-05-0) → tetraphenylantimony 4-hydroxybenzenesulfonate (209463-67-2)

Guidance literature:

In toluene; mixt. of Ph5Sb and Ph3Sb(OSO2C6H4(OH-4) in toluene stirred for 30 min; concd., cooled to -18°C, filtered off, washed (hexane), dried; elem. anal.;

DOI:10.1134/S1070328407030037

upstream raw materials:

p-hydoroxybenzenesulfonic acid

pentaphenylantimony

Refernces