Technology Process of l'(acetyl-2'-phenoxy)-3-tertiobutyldimethylsilyloxy-4-isochromanne
There total 3 articles about l'(acetyl-2'-phenoxy)-3-tertiobutyldimethylsilyloxy-4-isochromanne which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
1H-imidazole;
In
N,N-dimethyl-formamide;
for 3h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 80 percent / NaOCl, KH2PO4 / tetrahydrofuran; H2O / 0 deg C to RT
2: 22 percent / NaH / diethyl ether / 2 h / Ambient temperature
3: 71 percent / imidazole / dimethylformamide / 3 h / Ambient temperature
With
1H-imidazole; sodium hypochlorite; potassium dihydrogenphosphate; sodium hydride;
In
tetrahydrofuran; diethyl ether; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 22 percent / NaH / diethyl ether / 2 h / Ambient temperature
2: 71 percent / imidazole / dimethylformamide / 3 h / Ambient temperature
With
1H-imidazole; sodium hydride;
In
diethyl ether; N,N-dimethyl-formamide;
