chlorodimethyl(3-propyl)silane

Base Information

• Chemical Name: chlorodimethyl(3-propyl)silane
• CAS No.: 127801-36-9
• Molecular Formula: C₁₅H₂₃ClSi₂
• Molecular Weight: 294.972
• Mol file: 127801-36-9.mol

Synonyms:

Chemical Property of chlorodimethyl(3-propyl)silane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of chlorodimethyl(3-propyl)silane

There total 1 articles about chlorodimethyl(3-propyl)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3-bis(chlorodimethylsilyl)propane (2295-06-9) + phenylacetylene (536-74-3) → chlorodimethyl(3-propyl)silane (127801-36-9)

Guidance literature:

With ethylmagnesium bromide; Yield given. Multistep reaction; 1.) THF, 30 min, reflux; 2.) THF, 40-50 deg C;

DOI:10.1016/0022-328X(89)85001-6

Reference yield: 19.0%

chlorodimethyl(3-propyl)silane (127801-36-9) → dimethyl(phenylethynyl)<3-(dimethylsilyl)propyl>silane (127801-38-1)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 5h; Heating;

DOI:10.1016/0022-328X(89)85001-6

Reference yield:

chlorodimethyl(3-propyl)silane (127801-36-9) → 2-Benzylidene-1,1,3,3-tetramethyl-[1,3]disilinane

Guidance literature:

Multi-step reaction with 2 steps

1: 19 percent / lithium aluminum hydride / tetrahydrofuran / 5 h / Heating

2: 60.5 percent / chloroplatinic acid / cyclohexane; propan-2-ol / 1.) 3 h, reflux, 2.) 12 h, r.t.,

With lithium aluminium tetrahydride; dihydrogen hexachloroplatinate; In tetrahydrofuran; cyclohexane; isopropyl alcohol;

DOI:10.1016/0022-328X(89)85001-6

upstream raw materials:

1,3-bis(chlorodimethylsilyl)propane

phenylacetylene

Downstream raw materials:

dimethyl(phenylethynyl)<3-(dimethylsilyl)propyl>silane

Refernces