4-Chloro-3-methylaniline hydrochloride

Base Information

• Chemical Name: 4-Chloro-3-methylaniline hydrochloride
• CAS No.: 30273-23-5
• Molecular Formula: C7H8 Cl N . Cl H
• Molecular Weight: 178.061
• DSSTox Substance ID: DTXSID50184364
• Mol file: 30273-23-5.mol

Synonyms:4-chloro-3-methylaniline hydrochloride;30273-23-5;Benzenamine, 4-chloro-3-methyl-, hydrochloride (1:1);4-chloro-3-methylaniline;hydrochloride;4-Chloro-3-methylbenzenamine hydrochloride;SCHEMBL305574;DTXSID50184364;4-chloro-3-methylanilinehydrochloride;AKOS000104697;AS-0197;4-chloro-3-methyl-phenylamine hydrochloride;CS-0243723;EN300-267567;F72049;Benzenamine,4-chloro-3-methyl-,hydrochloride(1:1);Z2471262583

Chemical Property of 4-Chloro-3-methylaniline hydrochloride

Chemical Property:

• Vapor Pressure: 0.0358mmHg at 25°C
• Boiling Point: 241.5°Cat760mmHg
• Flash Point: 99.8°C
• PSA: 26.02000
• Density: g/cm³
• LogP: 3.61380
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 177.0112047
• Heavy Atom Count: 10
• Complexity: 94.9

Purity/Quality:

99% ^*data from raw suppliers

4-Chloro-3-methylanilinehydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=C(C=CC(=C1)N)Cl.Cl

Technology Process of 4-Chloro-3-methylaniline hydrochloride

There total 1 articles about 4-Chloro-3-methylaniline hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-chloro-2-methyl-4-nitrobenzene (13290-74-9) → 4-chloro-3-methyl-phenylamine hydrochloride (30273-23-5)

Guidance literature:

1-chloro-2-methyl-4-nitrobenzene; With iron; acetic acid; at 80 - 90 ℃; for 4h;

With hydrogenchloride; In 1,4-dioxane; water; at 100 ℃; for 3h;

Reference yield:

4-chloro-3-methyl-phenylamine hydrochloride (30273-23-5) → 6-chloro-toluene-3-sulfonyl chloride (6291-02-7)

Guidance literature:

4-chloro-3-methyl-phenylamine hydrochloride; With hydrogenchloride; acetic acid; sodium nitrite; In water; at -10 - -5 ℃; for 1h;

With sulfur dioxide; acetic acid; copper(l) chloride; In water; at 10 - 30 ℃; for 0.5h;

upstream raw materials:

1-chloro-2-methyl-4-nitrobenzene

Downstream raw materials:

6-chloro-toluene-3-sulfonyl chloride

Refernces