C₁₀H₁₅NO₃S

Base Information

• Chemical Name: C₁₀H₁₅NO₃S
• CAS No.: 1351416-49-3
• Molecular Formula: C₁₀H₁₅NO₃S
• Molecular Weight: 229.3
• Mol file: 1351416-49-3.mol

Synonyms:

Chemical Property of C₁₀H₁₅NO₃S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₀H₁₅NO₃S

There total 1 articles about C₁₀H₁₅NO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + C8H9NO5S (58443-49-5) → C10H15NO3S (1351416-49-3)

Guidance literature:

C₈H₉NO₅S; With palladium on activated charcoal; hydrogen;

formaldehyd; With palladium on activated charcoal; hydrogen;

DOI:10.1002/anie.201101801

Reference yield: 50.0%

C10H15NO3S (1351416-49-3) → C10H14ClNO2S (1351416-50-6)

Guidance literature:

C₁₀H₁₅NO₃S; With tetra-(n-butyl)ammonium iodide; sodium hydroxide; In dichloromethane; water; for 0.5h;

With bis(trichloromethyl) carbonate; N,N-dimethyl-formamide; In dichloromethane; for 5h;

DOI:10.1002/anie.201101801

Reference yield:

C10H15NO3S (1351416-49-3) → C10H14N4O2S (1351416-39-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: tetra-(n-butyl)ammonium iodide; sodium hydroxide / dichloromethane; water / 0.5 h

1.2: 5 h

2.1: sodium azide / water; acetone

With sodium azide; tetra-(n-butyl)ammonium iodide; sodium hydroxide; In dichloromethane; water; acetone;

DOI:10.1002/anie.201101801

upstream raw materials:

formaldehyd

C₈H₉NO₅S

Downstream raw materials:

C₁₀H₁₄N₄O₂S

C₁₀H₁₄ClNO₂S

Refernces