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heptanol-d16

Base Information Edit
  • Chemical Name:heptanol-d16
  • CAS No.:158778-86-0
  • Molecular Formula:C7H16O
  • Molecular Weight:132.076
  • Hs Code.:
  • Mol file:158778-86-0.mol
heptanol-d16

Synonyms:

Suppliers and Price of heptanol-d16
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of heptanol-d16 Edit
Chemical Property:
Purity/Quality:
Safty Information:
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Technology Process of heptanol-d16

There total 6 articles about heptanol-d16 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With lithium aluminium deuteride; In diethyl ether; for 8h; Heating;
Guidance literature:
Multi-step reaction with 3 steps
1: 1.) EtONa / 1.) EtOH, 50 deg C, 1 h, 2.) EtOH, 30 deg C, 6 h
2: 1.) D2O, NaOD, 2.) D2SO4 / 1.) reflux, 6 h, 2.) reflux, 4.5 h
3: 90.8 percent / LiAlD4 / diethyl ether / 8 h / Heating
With lithium aluminium deuteride; deuteriated sodium hydroxide; water-d2; sodium ethanolate; sulfuric acid-d2; In diethyl ether;
Guidance literature:
Multi-step reaction with 4 steps
1: 83.7 percent / red phosphorous, Br2 / 85 - 90 °C
2: 1.) EtONa / 1.) EtOH, 50 deg C, 1 h, 2.) EtOH, 30 deg C, 6 h
3: 1.) D2O, NaOD, 2.) D2SO4 / 1.) reflux, 6 h, 2.) reflux, 4.5 h
4: 90.8 percent / LiAlD4 / diethyl ether / 8 h / Heating
With phosphorus; lithium aluminium deuteride; deuteriated sodium hydroxide; bromine; water-d2; sodium ethanolate; sulfuric acid-d2; In diethyl ether;
upstream raw materials:

C7(2)H14O2

<(2)H11>Pentyl bromide

1-pentanol-d12

pentanoic acid-d10

Downstream raw materials:

n-heptyl-d15-bromide

Refernces Edit
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