Dihydroxy-acetic acid cyclohexyl ester

Base Information

• Chemical Name: Dihydroxy-acetic acid cyclohexyl ester
• CAS No.: 133017-23-9
• Molecular Formula: C₈H₁₄O₄
• Molecular Weight: 174.197
• Mol file: 133017-23-9.mol

Synonyms:

Chemical Property of Dihydroxy-acetic acid cyclohexyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Dihydroxy-acetic acid cyclohexyl ester

There total 3 articles about Dihydroxy-acetic acid cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dicyclohexyl trans-butenedioate (621-13-6,135607-72-6,47092-64-8) → Dihydroxy-acetic acid cyclohexyl ester (133017-23-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / piperidine, KMnO₄ / acetone / 1 h / Ambient temperature

2: H₅IO₆ / tetrahydrofuran / 4 h / Ambient temperature

With piperidine; potassium permanganate; periodic acid; In tetrahydrofuran; acetone;

Reference yield:

cyclohexanol (108-93-0) → Dihydroxy-acetic acid cyclohexyl ester (133017-23-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 73 percent / acidic ion exchange resin / CHCl₃ / 40 h / Heating

2: H₅IO₆ / tetrahydrofuran / 4 h / Ambient temperature

With acidic ion exchange resin; periodic acid; In tetrahydrofuran; chloroform;

Reference yield:

dicyclohexyl tartrate (15785-59-8,83071-79-8,133098-69-8,133098-70-1,140850-35-7) → cyclohexyl glyoxalate (133017-22-8) + Dihydroxy-acetic acid cyclohexyl ester (133017-23-9)

Guidance literature:

With periodic acid; In tetrahydrofuran; for 4h; Yield given. Title compound not separated from byproducts; Ambient temperature;

upstream raw materials:

dicyclohexyl tartrate

dicyclohexyl trans-butenedioate

cyclohexanol

Refernces