2,3-anhydro-N,N-dibenzyl-5-O-benzyl-4,6-O-ethylidene-D-altro-hexonamide

Base Information

• Chemical Name: 2,3-anhydro-N,N-dibenzyl-5-O-benzyl-4,6-O-ethylidene-D-altro-hexonamide
• CAS No.: 1030598-09-4
• Molecular Formula: C₂₉H₃₁NO₅
• Molecular Weight: 473.569
• Mol file: 1030598-09-4.mol

Synonyms:

Chemical Property of 2,3-anhydro-N,N-dibenzyl-5-O-benzyl-4,6-O-ethylidene-D-altro-hexonamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3-anhydro-N,N-dibenzyl-5-O-benzyl-4,6-O-ethylidene-D-altro-hexonamide

There total 1 articles about 2,3-anhydro-N,N-dibenzyl-5-O-benzyl-4,6-O-ethylidene-D-altro-hexonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl bromide (100-39-0) + (1'R)-(-)-2,4-O-ethylidene-D-erythrose (70377-89-8,315216-23-0) + (N,N-dibenzylcarbamoylmethylene)dimethyl sulfurane → 2,3-anhydro-N,N-dibenzyl-5-O-benzyl-4,6-O-ethylidene-D-altro-hexonamide (1030598-09-4) + 2,3-anhydro-N,N-dibenzyl-5-O-benzyl-4,6-O-ethylidene-D-gluco-hexonamide

Guidance literature:

(1'R)-(-)-2,4-O-ethylidene-D-erythrose; (N,N-dibenzylcarbamoylmethylene)dimethyl sulfurane; With sodium hydroxide; In dichloromethane; at 20 ℃; for 0.5h;

benzyl bromide; With tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; Further stages. Title compound not separated from byproducts.;

DOI:10.1016/j.tetasy.2008.02.003

upstream raw materials:

benzyl bromide

(1'R)-(-)-2,4-O-ethylidene-D-erythrose

Refernces