4-N-isopropylamino-3,4'-dinitroazobenzene

Base Information

• Chemical Name: 4-N-isopropylamino-3,4'-dinitroazobenzene
• CAS No.: 1393133-95-3
• Molecular Formula: C₁₅H₁₅N₅O₄
• Molecular Weight: 329.315
• Mol file: 1393133-95-3.mol

Synonyms:

Chemical Property of 4-N-isopropylamino-3,4'-dinitroazobenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-N-isopropylamino-3,4'-dinitroazobenzene

There total 3 articles about 4-N-isopropylamino-3,4'-dinitroazobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

4-fluoro-3,4'-dinitroazobenzene (1393133-94-2) + isopropylamine (75-31-0) → 4-N-isopropylamino-3,4'-dinitroazobenzene (1393133-95-3)

Guidance literature:

In toluene; at 80 ℃; for 20h;

DOI:10.1039/c2nj40313g

Reference yield:

4-nitrosonitrobenzene (4485-08-9) → 4-N-isopropylamino-3,4'-dinitroazobenzene (1393133-95-3)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid / 12 h

2: toluene / 20 h / 80 °C

With acetic acid; In toluene;

DOI:10.1039/c2nj40313g

Reference yield:

4-Nitro-N-phenylhydroxylamine (16169-16-7) → 4-N-isopropylamino-3,4'-dinitroazobenzene (1393133-95-3)

Guidance literature:

Multi-step reaction with 3 steps

1: nitric acid

2: acetic acid / 12 h

3: toluene / 20 h / 80 °C

With nitric acid; acetic acid; In toluene;

DOI:10.1039/c2nj40313g

upstream raw materials:

4-fluoro-3,4'-dinitroazobenzene

isopropylamine

4-nitrosonitrobenzene

4-Nitro-N-phenylhydroxylamine

Refernces