(E)-3-Amino-4,4,4-trichloro-2-cyano-but-2-enoic acid phenyl ester

Base Information

• Chemical Name: (E)-3-Amino-4,4,4-trichloro-2-cyano-but-2-enoic acid phenyl ester
• CAS No.: 55655-42-0
• Molecular Formula: C₁₁H₇Cl₃N₂O₂
• Molecular Weight: 305.548
• Mol file: 55655-42-0.mol

Synonyms:

Chemical Property of (E)-3-Amino-4,4,4-trichloro-2-cyano-but-2-enoic acid phenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (E)-3-Amino-4,4,4-trichloro-2-cyano-but-2-enoic acid phenyl ester

There total 1 articles about (E)-3-Amino-4,4,4-trichloro-2-cyano-but-2-enoic acid phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenyl 2-cyanoacetate (6131-48-2) + trichloroacetonitrile (545-06-2) → (E)-3-Amino-4,4,4-trichloro-2-cyano-but-2-enoic acid phenyl ester (55655-42-0)

Guidance literature:

With sodium acetate; In methanol;

Reference yield:

(E)-3-Amino-4,4,4-trichloro-2-cyano-but-2-enoic acid phenyl ester (55655-42-0) → β-Cyano-β-phenoxycarbonyl-α-amino-α-hydrazinoethylen

Guidance literature:

With hydrazine hydrate; In N,N-dimethyl-formamide;

Reference yield:

(E)-3-Amino-4,4,4-trichloro-2-cyano-but-2-enoic acid phenyl ester (55655-42-0) → C11H6Cl4N2O2 (55655-49-7)

Guidance literature:

With phosphorus pentachloride;

upstream raw materials:

phenyl 2-cyanoacetate

trichloroacetonitrile

Downstream raw materials:

C₁₁H₆Cl₄N₂O₂