Technology Process of Magnesium, bromo[(4-chlorophenyl)methyl]-
There total 1 articles about Magnesium, bromo[(4-chlorophenyl)methyl]- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
magnesium;
In
diethyl ether;
at 20 ℃;
for 0.75h;
- Guidance literature:
-
4-chlorobenzylmagnesium bromide;
With
copper(I) bromide dimethylsulfide complex;
In
tetrahydrofuran;
at -78 ℃;
for 0.166667h;
(3aR,6aR)-2,2-Dimethyl-3a,6a-dihydro-cyclopenta[1,3]dioxol-4-one;
With
N,N,N,N,N,N-hexamethylphosphoric triamide; chloro-trimethyl-silane;
In
tetrahydrofuran;
at -78 ℃;
for 3h;
Inert atmosphere;
- Guidance literature:
-
In
diethyl ether; benzene;
at 35 - 40 ℃;
for 2h;