Technology Process of 4,4'-hexafluoroisopropylidenebis[4-(N,N-diphenylamino)phenyl phthalimide]
There total 4 articles about 4,4'-hexafluoroisopropylidenebis[4-(N,N-diphenylamino)phenyl phthalimide] which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: palladium on activated charcoal; hydrazine hydrate / ethanol / 12 h / Reflux
2.1: tetrahydrofuran / 1 h / Inert atmosphere
2.2: 4 h / Reflux
With
palladium on activated charcoal; hydrazine hydrate;
In
tetrahydrofuran; ethanol;
DOI:10.1021/cm201665g
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / N,N-dimethyl acetamide / 0.5 h / 20 °C
1.2: 1 h / 100 °C
2.1: palladium on activated charcoal; hydrazine hydrate / ethanol / 12 h / Reflux
3.1: tetrahydrofuran / 1 h / Inert atmosphere
3.2: 4 h / Reflux
With
palladium on activated charcoal; sodium hydride; hydrazine hydrate;
In
tetrahydrofuran; ethanol; N,N-dimethyl acetamide;
DOI:10.1021/cm201665g
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / N,N-dimethyl acetamide / 0.5 h / 20 °C
1.2: 1 h / 100 °C
2.1: palladium on activated charcoal; hydrazine hydrate / ethanol / 12 h / Reflux
3.1: tetrahydrofuran / 1 h / Inert atmosphere
3.2: 4 h / Reflux
With
palladium on activated charcoal; sodium hydride; hydrazine hydrate;
In
tetrahydrofuran; ethanol; N,N-dimethyl acetamide;
DOI:10.1021/cm201665g
