Technology Process of C22H24N2O7
There total 5 articles about C22H24N2O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate / acetone / Reflux
2.1: silver nitrate / acetonitrile / 3 h / 70 °C
3.1: potassium permanganate / acetone / 10 h / Reflux
4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.5 h / 20 °C
4.2: 20 °C
With
potassium permanganate; potassium carbonate; silver nitrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane; acetone; acetonitrile;
DOI:10.1016/j.bmcl.2013.02.035
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium permanganate / acetone / 10 h / Reflux
2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.5 h / 20 °C
2.2: 20 °C
With
potassium permanganate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane; acetone;
DOI:10.1016/j.bmcl.2013.02.035
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium nitrate; sulfuric acid / 12 h / 20 °C
2.1: iron; ammonium chloride / water; tetrahydrofuran / 2 h / 65 °C
3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.5 h / 20 °C
3.2: 20 °C
With
sulfuric acid; iron; ammonium chloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium nitrate;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.bmcl.2013.02.035
