N-methoxy-1,1-bis(4-methylphenyl)methanimine

Base Information

• Chemical Name: N-methoxy-1,1-bis(4-methylphenyl)methanimine
• CAS No.: 65311-13-9
• Molecular Formula: C16H17 N O
• Molecular Weight: 239.317
• Mol file: 65311-13-9.mol

Synonyms:4,4'-DimethylbenzophenoneO-methyloxime; NSC 146535

Chemical Property of N-methoxy-1,1-bis(4-methylphenyl)methanimine

Chemical Property:

• Vapor Pressure: 0.00016mmHg at 25°C
• Boiling Point: 341.4°C at 760 mmHg
• Flash Point: 130.7°C
• Density: 0.98g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-methoxy-1,1-bis(4-methylphenyl)methanimine

There total 1 articles about N-methoxy-1,1-bis(4-methylphenyl)methanimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 4,4'-dimethylbenzophenone-o-methyloxime (65311-13-9)

Guidance literature:

4,4'-Dimethylbenzophenon-oxim, CH3I, Ag2O;

DOI:10.1021/jo00404a010

Reference yield: 98.0%

4,4'-dimethylbenzophenone-o-methyloxime (65311-13-9) → C16H17NO2

Guidance literature:

With Oxone; palladium diacetate; triphenylphosphine; In 1,1,2,2-tetrachloroethane; at 80 ℃; for 24h;

DOI:10.1021/acscatal.5b01700

Reference yield: 72.0%

4,4'-dimethylbenzophenone-o-methyloxime (65311-13-9) + 3-phenyl-5H-1,4,2-dioxazol-5-one (19226-36-9) → N-(2-((methoxyimino)(m-tolyl)methyl)-4-methylphenyl)benzamide

Guidance literature:

With bromopentacarbonylmanganese(I); at 50 ℃; for 4h; Ionic liquid;

DOI:10.1016/j.tetlet.2019.151521