Benzoic acid, 4-propoxy-, propyl ester

Base Information

• Chemical Name: Benzoic acid, 4-propoxy-, propyl ester
• CAS No.: 111222-67-4
• Molecular Formula: C₁₃H₁₈O₃
• Molecular Weight: 222.284
• Mol file: 111222-67-4.mol

Synonyms:

Chemical Property of Benzoic acid, 4-propoxy-, propyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 4-propoxy-, propyl ester

There total 3 articles about Benzoic acid, 4-propoxy-, propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

propan-1-ol (71-23-8) + carbon monoxide (201230-82-2) + para-chloroacetophenone (99-91-2) → terephthalic acid dipropyl ester (1962-74-9) + propyl 4-chloro benzoate (25800-30-0) + 4-propoxy-benzoic acid propyl ester (111222-67-4) + 4-acetyl-benzoic acid propyl ester

Guidance literature:

With potassium tert-butylate; palladium dichloride; 1,2-bis[di(t-butyl)phosphinomethyl]benzene; at 100 ℃; for 48h; under 15001.2 Torr; Further byproducts given;

DOI:10.1039/b501868d

Reference yield:

4-hydroxy-benzoic acid (99-96-7) → 4-propoxy-benzoic acid propyl ester (111222-67-4)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogen chloride / Erwaermen des mit Schwefelsaeure versetzten Reaktionsgemisches

2: potassium carbonate; acetone

With hydrogenchloride; potassium carbonate; acetone;

DOI:10.1002/ardp.19382760305

Reference yield:

nipasol (94-13-3) + propyl bromide (106-94-5) → 4-propoxy-benzoic acid propyl ester (111222-67-4)

Guidance literature:

With potassium carbonate; acetone;

DOI:10.1002/ardp.19382760305

upstream raw materials:

nipasol

propyl bromide

propan-1-ol

carbon monoxide

Refernces